TA Instruments

sacha desengrasada-0023f

27/04/2022 1:06:20 p. m.

Sample name	sacha desengrasada
Sample notes	 
Experiment notes	
Operator	Default User
Sample density	1,000 g/cm^3
Results file name	sacha desengrasada
Run number	23 
Results directory	C:\Ta\Data\Ar1500\Ar1500\DIEGO ROA
Experiment was run on	27/04/2022 1:06:20 p. m.

Procedure name	Oscillation procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	50,0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Perform pre-shear	No
Perform equilibration	No
Wait for zero velocity	No
Purge gas only	No

Step name	Conditioning Step 2
Step notes	
Perform step	Yes
Initial temperature	50,0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Perform pre-shear	Yes
Pre-shear variable	12,00 rad/s
Pre-shear duration	0:00:10 hh:mm:ss
Motor mode	auto 
Perform equilibration	Yes
Equilibration duration	0:04:00 hh:mm:ss
Wait for zero velocity	No
Purge gas only	No

Step name	Peak hold step 1
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 16,75 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:02 hh:mm:ss
Temperature	50,0 C
Wait for temperature	No
Motor mode	auto 

Step name	Temperature ramp step 1
Step notes	
Perform step	Yes
Ramp type	Temperature ramp
Start temperature	50,0 C
End temperature	90,0 C
Wait for start temperature	No
Ramp rate	12,66 C/min
Delay time	0:00:02 hh:mm:ss
Controlled variable	velocity 16,75 rad/s
Motor mode	auto 

Step name	Peak hold step 2
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 16,75 rad/s
Duration	0:05:00 hh:mm:ss
Delay time	0:00:02 hh:mm:ss
Temperature	90,0 C
Wait for temperature	No
Motor mode	auto 

Step name	Temperature ramp step 2
Step notes	
Perform step	Yes
Ramp type	Temperature ramp
Start temperature	90,0 C
End temperature	50,0 C
Wait for start temperature	No
Ramp rate	12,66 C/min
Delay time	0:00:02 hh:mm:ss
Controlled variable	velocity 16,75 rad/s
Motor mode	auto 

Step name	Peak hold step 3
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 16,75 rad/s
Duration	0:02:00 hh:mm:ss
Delay time	0:00:02 hh:mm:ss
Temperature	50,0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	shear stress 0,1000 Pa
End controlled variable	shear stress 100,0 Pa
Duration	0:05:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:10 hh:mm:ss
Temperature	30,0 C
Wait for temperature	No
Match duration and start value to previous step	No
Oversampling	Yes

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	30,0 C
Set temperature system idle	No

Geometry name	Starch cell
Geometry notes	Starch cell
Geometry material	High temperature
gap	5500 micro m
Calibration factor	10800 
Gap offset	0 micro m
Geometry inertia	2,152 micro N.m.s^2
Shear rate factor	1,000 
Shear stress factor	10800 1/m^3
Measurement system factor	10800 1/m^3
Fluid density factor	1,000E-15 m^5
Normal force factor	1,000 1/m^2
Backoff distance	1,25E5 micro m

Gap zero mode	Standard
Sample compression	none 
Compression distance	1000,0 micro m
Compression velocity	100,0 micro m/s
Fine velocity	1000,0 micro m/s
Coarse velocity	3000,0 micro m/s
Other velocity	3000,0 micro m/s
Current temperature system	Starch cell
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	5,0 C
Cooling water range	15,0 C
Bearing friction correction	Yes
Bearing friction	1,222 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1,0000 , offset 0 C
	Water bath - span 1,0000 , offset 0 C
	Torsion oven - plate - span 1,0000 , offset 0 C
	Torsion oven - solid sample - span 1,0000 , offset 0 C
	Peltier concentric cylinders - span 1,0000 , offset 0 C
	None - span 1,0000 , offset 0 C
	Stress relaxation - span 1,0000 , offset 0 C
	Current temperature system - span 1,0000 , offset 0 C
Bearing mapping type	fast 
Number of mapping iterations	1
Instrument type (MType)	AR1500ex
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	172.23.191.2
Software version	V5.8.2
Windows version	Windows XP 6.2
Instrument inertia	15,97 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0,2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0,1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	3,000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	No
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	No
Creep zero displacement	Yes
Store images to the results for creep steps	No
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	No
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	No
Flow torque limit	10,00 micro N.m
Flow velocity limit	1,000E-3 rad/s
Oscillation torque limit	5,00 micro N.m
Oscillation displacement limit	1,00E-5 rad
Oscillation raw phase limit	170,0 degrees
Oscillation minimum normal force limit	0 N
Oscillation maximum normal force limit	0 N
Flow velocity tolerance	5,00 %
Oscillation torque tolerance	1,00 %
Oscillation displacement tolerance	5,00 %
Oscillation velocity tolerance	5,00 %
Temperature tolerance	1,0 C

Peak hold step 1

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

2,747	16,75	0,1640	2,0040	50,0	0
2,384	16,75	0,1423	4,0080	50,0	0
2,482	16,75	0,1482	6,0080	49,9	0
2,618	16,75	0,1563	8,0080	49,9	0
2,691	16,75	0,1607	10,012	49,8	0
2,682	16,75	0,1601	12,016	49,7	0
2,670	16,75	0,1594	14,012	49,7	0
2,699	16,75	0,1612	16,028	49,6	0
2,682	16,75	0,1601	18,028	49,7	0
2,675	16,75	0,1597	20,012	49,7	0
2,703	16,75	0,1614	22,016	49,8	0
2,681	16,75	0,1601	24,012	49,8	0
2,669	16,75	0,1593	26,016	49,9	0
2,697	16,75	0,1610	28,012	50,0	0
2,698	16,75	0,1611	30,012	50,0	0

Temperature ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

2,686	16,75	0,1604	1,9920	50,1	0
2,662	16,75	0,1589	3,9920	50,1	0
2,695	16,75	0,1609	6,0040	50,1	0
2,687	16,75	0,1604	7,9840	50,2	0
2,670	16,75	0,1594	9,9840	50,2	0
2,673	16,75	0,1596	11,984	50,3	0
2,661	16,75	0,1588	13,992	50,5	0
2,663	16,75	0,1590	15,992	50,6	0
2,665	16,75	0,1591	18,008	50,9	0
2,648	16,75	0,1581	19,992	51,1	0
2,657	16,75	0,1587	22,012	51,4	0
2,634	16,75	0,1572	24,000	51,7	0
2,620	16,75	0,1564	25,996	52,1	0
2,594	16,75	0,1549	27,984	52,5	0
2,589	16,75	0,1546	29,984	52,9	0
2,575	16,75	0,1537	31,988	53,4	0
2,547	16,75	0,1520	34,000	53,8	0
2,515	16,75	0,1501	35,984	54,2	0
2,504	16,75	0,1495	37,988	54,7	0
2,479	16,75	0,1480	39,984	55,2	0
2,468	16,75	0,1473	41,984	55,7	0
2,468	16,75	0,1473	43,996	56,1	0
2,438	16,75	0,1456	45,996	56,6	0
2,416	16,75	0,1442	47,980	57,0	0
2,414	16,75	0,1441	49,980	57,5	0
2,380	16,75	0,1421	51,988	58,0	0
2,361	16,75	0,1409	53,988	58,5	0
2,349	16,75	0,1402	55,988	58,9	0
2,335	16,75	0,1394	57,988	59,4	0
2,310	16,75	0,1379	60,004	59,8	0
2,305	16,75	0,1376	62,000	60,3	0
2,294	16,75	0,1369	64,000	60,7	0
2,276	16,75	0,1359	65,984	61,2	0
2,287	16,75	0,1365	67,988	61,7	0
2,265	16,75	0,1352	69,988	62,1	0
2,258	16,75	0,1348	71,988	62,5	0
2,242	16,75	0,1338	73,984	63,0	0
2,228	16,75	0,1330	76,000	63,4	0
2,234	16,75	0,1334	77,988	63,9	0
2,224	16,75	0,1328	79,992	64,4	0
2,214	16,75	0,1322	81,992	64,9	0
2,203	16,75	0,1315	83,992	65,3	0
2,198	16,75	0,1312	85,992	65,7	0
2,188	16,75	0,1306	87,996	66,2	0
2,178	16,75	0,1300	89,980	66,6	0
2,189	16,75	0,1307	91,980	67,0	0
2,192	16,75	0,1309	93,984	67,5	0
2,183	16,75	0,1303	95,984	67,9	0
2,178	16,75	0,1301	97,984	68,4	0
2,181	16,75	0,1302	99,984	68,8	0
2,186	16,75	0,1305	101,99	69,2	0
2,189	16,75	0,1307	103,98	69,7	0
2,195	16,75	0,1311	105,98	70,1	0
2,207	16,75	0,1318	107,98	70,5	0
2,211	16,75	0,1320	109,98	71,0	0
2,242	16,75	0,1338	111,98	71,4	0
2,272	16,75	0,1356	113,99	71,9	0
2,281	16,75	0,1362	115,98	72,2	0
2,312	16,75	0,1380	117,98	72,7	0
2,361	16,75	0,1409	120,00	73,2	0
2,379	16,75	0,1420	121,98	73,6	0
2,451	16,75	0,1463	123,99	74,1	0
2,514	16,75	0,1501	125,99	74,5	0
2,544	16,75	0,1519	127,99	74,9	0
2,615	16,75	0,1561	129,99	75,4	0
2,706	16,75	0,1615	131,99	75,8	0
2,779	16,75	0,1659	133,99	76,3	0
2,914	16,75	0,1740	135,99	76,7	0
3,046	16,75	0,1819	137,99	77,1	0
3,183	16,75	0,1900	139,99	77,6	0
3,348	16,75	0,1999	141,99	77,9	0
3,582	16,75	0,2139	143,99	78,3	0
3,700	16,75	0,2209	145,99	78,8	0
3,950	16,75	0,2359	147,99	79,1	0
4,237	16,75	0,2530	149,99	79,6	0
4,487	16,75	0,2679	151,99	80,0	0
4,811	16,75	0,2872	153,99	80,4	0
5,138	16,75	0,3067	155,99	80,8	0
5,418	16,75	0,3235	157,99	81,3	0
5,894	16,75	0,3519	159,99	81,8	0
6,323	16,75	0,3775	162,00	82,3	0
6,686	16,75	0,3992	164,00	82,7	0
7,129	16,75	0,4256	165,98	83,2	0
7,437	16,75	0,4440	167,98	83,6	0
7,568	16,75	0,4518	169,98	84,1	0
7,930	16,75	0,4734	171,98	84,5	0
7,971	16,75	0,4759	173,98	84,9	0
7,844	16,75	0,4683	175,99	85,3	0
7,690	16,75	0,4590	177,98	85,7	0
7,537	16,75	0,4500	179,99	86,1	0
7,462	16,75	0,4455	181,99	86,6	0
7,251	16,75	0,4329	183,99	86,9	0
7,023	16,75	0,4193	185,99	87,4	0
6,903	16,75	0,4122	187,99	87,7	0
6,684	16,75	0,3990	189,99	88,2	0

Peak hold step 2

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

6,574	16,75	0,3925	2,0040	88,6	0
6,387	16,75	0,3813	3,9920	89,0	0
6,282	16,75	0,3751	6,0040	89,5	0
6,185	16,75	0,3692	7,9920	89,8	0
6,210	16,75	0,3708	10,008	90,2	0
6,141	16,75	0,3666	12,008	90,5	0
6,210	16,75	0,3708	14,012	90,8	0
6,263	16,75	0,3738	16,008	91,0	0
6,295	16,75	0,3758	18,008	91,2	0
6,288	16,75	0,3754	20,008	91,4	0
6,284	16,75	0,3751	22,008	91,5	0
6,233	16,75	0,3721	23,992	91,5	0
6,197	16,75	0,3700	26,008	91,6	0
6,052	16,75	0,3613	28,008	91,6	0
5,957	16,75	0,3557	30,024	91,6	0
5,848	16,75	0,3491	31,996	91,6	0
5,799	16,75	0,3462	34,008	91,5	0
5,764	16,75	0,3441	36,008	91,3	0
5,680	16,75	0,3391	38,008	91,0	0
5,629	16,75	0,3361	40,000	90,6	0
5,542	16,75	0,3308	42,012	90,2	0
5,455	16,75	0,3257	43,996	89,9	0
5,343	16,75	0,3190	46,000	89,6	0
5,232	16,75	0,3123	48,636	89,4	0
5,117	16,75	0,3055	50,012	89,3	0
5,015	16,75	0,2994	52,004	89,3	0
4,895	16,75	0,2922	53,992	89,4	0
4,787	16,75	0,2858	55,996	89,4	0
4,723	16,75	0,2820	58,000	89,5	0
4,640	16,75	0,2770	60,000	89,6	0
4,557	16,75	0,2720	62,004	89,7	0
4,472	16,75	0,2670	63,996	89,8	0
4,437	16,75	0,2649	65,992	89,9	0
4,368	16,75	0,2607	67,996	90,0	0
4,348	16,75	0,2596	69,996	90,1	0
4,329	16,75	0,2584	72,000	90,2	0
4,257	16,75	0,2542	74,000	90,3	0
4,244	16,75	0,2534	76,004	90,3	0
4,215	16,75	0,2517	78,004	90,3	0
4,189	16,75	0,2501	79,992	90,4	0
4,149	16,75	0,2477	81,996	90,4	0
4,165	16,75	0,2486	84,000	90,4	0
4,132	16,75	0,2467	86,004	90,4	0
4,097	16,75	0,2446	88,008	90,5	0
4,080	16,75	0,2436	89,988	90,5	0
4,077	16,75	0,2434	91,992	90,5	0
4,046	16,75	0,2416	93,992	90,5	0
4,054	16,75	0,2420	95,996	90,6	0
4,034	16,75	0,2409	98,000	90,6	0
4,022	16,75	0,2401	100,00	90,6	0
4,013	16,75	0,2396	102,00	90,6	0
4,000	16,75	0,2388	104,00	90,6	0
3,993	16,75	0,2384	106,01	90,6	0
3,988	16,75	0,2381	108,00	90,6	0
4,007	16,75	0,2392	109,99	90,5	0
3,997	16,75	0,2386	112,00	90,5	0
3,972	16,75	0,2371	114,00	90,6	0
3,933	16,75	0,2348	116,00	90,6	0
3,979	16,75	0,2375	117,99	90,6	0
3,940	16,75	0,2352	119,99	90,6	0
3,932	16,75	0,2347	122,00	90,6	0
3,906	16,75	0,2332	124,00	90,6	0
3,934	16,75	0,2348	126,00	90,6	0
3,910	16,75	0,2334	128,00	90,6	0
3,906	16,75	0,2332	129,99	90,5	0
3,911	16,75	0,2335	131,99	90,5	0
3,922	16,75	0,2341	134,00	90,5	0
3,910	16,75	0,2334	136,00	90,4	0
3,917	16,75	0,2338	138,00	90,4	0
3,906	16,75	0,2332	139,99	90,4	0
3,917	16,75	0,2339	141,99	90,4	0
3,910	16,75	0,2334	143,99	90,3	0
3,889	16,75	0,2322	146,00	90,3	0
3,867	16,75	0,2309	148,00	90,3	0
3,885	16,75	0,2319	149,99	90,3	0
3,887	16,75	0,2321	152,00	90,3	0
3,853	16,75	0,2300	154,00	90,2	0
3,868	16,75	0,2309	156,00	90,2	0
3,868	16,75	0,2309	158,00	90,2	0
3,889	16,75	0,2322	160,02	90,2	0
3,878	16,75	0,2315	162,00	90,2	0
3,860	16,75	0,2304	163,99	90,1	0
3,854	16,75	0,2301	165,99	90,1	0
3,864	16,75	0,2307	167,99	90,1	0
3,843	16,75	0,2294	169,99	90,1	0
3,841	16,75	0,2293	172,00	90,0	0
3,838	16,75	0,2291	174,00	90,0	0
3,876	16,75	0,2314	176,00	90,0	0
3,834	16,75	0,2289	178,01	90,0	0
3,817	16,75	0,2279	179,99	90,0	0
3,823	16,75	0,2283	181,99	90,0	0
3,837	16,75	0,2291	184,01	90,0	0
3,830	16,75	0,2287	186,00	90,0	0
3,792	16,75	0,2264	188,00	90,0	0
3,812	16,75	0,2276	190,01	90,0	0
3,795	16,75	0,2266	192,02	90,0	0
3,808	16,75	0,2273	194,00	90,0	0
3,783	16,75	0,2259	196,01	90,0	0
3,812	16,75	0,2276	197,99	90,0	0
3,797	16,75	0,2267	200,00	90,0	0
3,800	16,75	0,2269	202,00	90,0	0
3,806	16,75	0,2272	204,00	90,0	0
3,781	16,75	0,2257	206,00	90,0	0
3,788	16,75	0,2261	208,00	90,0	0
3,773	16,75	0,2253	210,00	90,0	0
3,797	16,75	0,2267	212,01	90,0	0
3,774	16,75	0,2253	214,00	90,0	0
3,785	16,75	0,2260	216,00	90,0	0
3,787	16,75	0,2261	218,00	90,0	0
3,767	16,75	0,2249	219,99	90,0	0
3,750	16,75	0,2239	221,99	90,0	0
3,778	16,75	0,2256	224,00	90,0	0
3,760	16,75	0,2245	226,00	90,0	0
3,766	16,75	0,2249	228,00	90,0	0
3,759	16,75	0,2244	230,00	90,0	0
3,766	16,75	0,2248	231,99	90,0	0
3,758	16,75	0,2243	234,00	90,0	0
3,762	16,75	0,2246	235,99	90,0	0
3,782	16,75	0,2258	238,00	90,0	0
3,756	16,75	0,2242	240,00	90,0	0
3,741	16,75	0,2234	242,00	90,0	0
3,728	16,75	0,2226	244,00	90,0	0
3,755	16,75	0,2242	246,00	90,0	0
3,739	16,75	0,2232	248,00	90,0	0
3,744	16,75	0,2235	250,00	90,0	0
3,742	16,75	0,2234	252,00	90,0	0
3,742	16,75	0,2234	254,01	90,0	0
3,748	16,75	0,2238	255,99	90,0	0
3,743	16,75	0,2235	258,00	90,0	0
3,761	16,75	0,2245	260,00	90,0	0
3,741	16,75	0,2233	262,00	90,0	0
3,732	16,75	0,2228	264,00	90,0	0
3,726	16,75	0,2224	266,00	90,0	0
3,737	16,75	0,2231	268,00	90,0	0
3,740	16,75	0,2233	269,99	90,0	0
3,735	16,75	0,2230	272,00	90,0	0
3,726	16,75	0,2225	274,01	90,0	0
3,736	16,75	0,2231	276,00	90,0	0
3,743	16,75	0,2234	278,00	90,0	0
3,716	16,75	0,2218	280,00	90,0	0
3,718	16,75	0,2219	282,00	90,0	0
3,734	16,75	0,2229	284,00	90,0	0
3,745	16,75	0,2236	286,00	90,0	0
3,725	16,75	0,2224	287,99	90,0	0
3,764	16,75	0,2247	289,99	90,0	0
3,713	16,75	0,2216	292,00	90,0	0
3,723	16,75	0,2223	294,01	90,0	0
3,724	16,75	0,2224	296,01	90,0	0
3,742	16,75	0,2234	298,01	90,0	0
3,713	16,75	0,2216	300,00	90,0	0

Temperature ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

3,704	16,75	0,2211	1,9960	90,0	0
3,725	16,75	0,2224	3,9960	90,0	0
3,711	16,75	0,2216	6,0040	90,0	0
3,721	16,75	0,2221	8,0000	90,0	0
3,747	16,75	0,2237	10,000	90,0	0
3,748	16,75	0,2238	12,000	89,9	0
3,736	16,75	0,2230	13,988	89,8	0
3,850	16,75	0,2298	16,004	89,5	0
3,897	16,75	0,2327	17,992	88,9	0
3,958	16,75	0,2363	19,992	88,0	0
3,994	16,75	0,2384	21,996	87,3	0
4,006	16,75	0,2391	23,996	86,6	0
4,041	16,75	0,2413	25,996	86,2	0
4,071	16,75	0,2430	28,000	85,8	0
4,089	16,75	0,2441	30,000	85,6	0
4,118	16,75	0,2458	31,988	85,4	0
4,165	16,75	0,2487	33,988	85,1	0
4,192	16,75	0,2502	35,992	84,9	0
4,195	16,75	0,2505	37,992	84,7	0
4,219	16,75	0,2519	40,012	84,4	0
4,258	16,75	0,2542	41,996	84,2	0
4,285	16,75	0,2559	43,996	83,9	0
4,330	16,75	0,2585	46,000	83,3	0
4,375	16,75	0,2612	47,992	82,7	0
4,424	16,75	0,2641	49,992	81,9	0
4,455	16,75	0,2659	51,992	81,3	0
4,479	16,75	0,2674	54,000	80,8	0
4,490	16,75	0,2681	56,000	80,5	0
4,531	16,75	0,2705	57,988	80,2	0
4,543	16,75	0,2712	59,992	79,9	0
4,553	16,75	0,2718	62,012	79,7	0
4,604	16,75	0,2749	63,992	79,4	0
4,616	16,75	0,2756	65,996	79,0	0
4,674	16,75	0,2791	67,996	78,4	0
4,729	16,75	0,2823	70,000	77,7	0
4,736	16,75	0,2827	72,000	76,9	0
4,780	16,75	0,2854	74,004	76,4	0
4,803	16,75	0,2867	75,992	76,0	0
4,832	16,75	0,2885	77,996	75,7	0
4,801	16,75	0,2866	79,996	75,4	0
4,849	16,75	0,2895	82,000	75,2	0
4,883	16,75	0,2915	83,992	75,0	0
4,909	16,75	0,2930	85,992	74,7	0
4,942	16,75	0,2950	88,000	74,2	0
4,955	16,75	0,2958	90,000	73,5	0
5,013	16,75	0,2993	91,988	72,9	0
5,055	16,75	0,3018	93,992	72,1	0
5,084	16,75	0,3035	95,996	71,7	0
5,104	16,75	0,3047	98,000	71,3	0
5,161	16,75	0,3081	100,01	71,0	0
5,180	16,75	0,3093	102,00	70,7	0
5,179	16,75	0,3092	104,00	70,5	0
5,243	16,75	0,3130	106,01	70,2	0
5,268	16,75	0,3145	108,00	69,9	0
5,308	16,75	0,3169	110,01	69,3	0
5,343	16,75	0,3190	112,00	68,6	0
5,430	16,75	0,3241	114,00	68,1	0
5,462	16,75	0,3261	116,00	67,5	0
5,502	16,75	0,3285	118,00	67,1	0
5,506	16,75	0,3287	120,00	66,7	0
5,543	16,75	0,3309	122,02	66,4	0
5,616	16,75	0,3353	124,00	66,1	0
5,597	16,75	0,3341	126,01	65,9	0
5,667	16,75	0,3383	128,00	65,4	0
5,721	16,75	0,3416	130,01	65,0	0
5,770	16,75	0,3445	131,99	64,4	0
5,841	16,75	0,3487	133,99	63,8	0
5,874	16,75	0,3507	135,99	63,2	0
5,939	16,75	0,3546	138,00	62,8	0
5,975	16,75	0,3567	140,00	62,5	0
6,008	16,75	0,3587	142,00	62,1	0
6,071	16,75	0,3624	144,00	61,8	0
6,088	16,75	0,3634	146,00	61,6	0
6,164	16,75	0,3680	148,01	61,2	0
6,256	16,75	0,3735	150,00	60,6	0
6,295	16,75	0,3758	152,01	60,1	0
6,371	16,75	0,3804	154,00	59,5	0
6,398	16,75	0,3820	156,01	59,0	0
6,537	16,75	0,3903	158,00	58,6	0
6,558	16,75	0,3915	159,98	58,2	0
6,604	16,75	0,3943	161,99	57,9	0
6,701	16,75	0,4000	163,99	57,5	0
6,728	16,75	0,4016	165,99	57,1	0
6,839	16,75	0,4083	168,00	56,7	0
6,860	16,75	0,4095	170,00	56,3	0
6,971	16,75	0,4162	171,99	55,8	0
7,040	16,75	0,4203	173,99	55,4	0
7,105	16,75	0,4242	176,00	54,9	0
7,275	16,75	0,4343	178,00	54,4	0
7,289	16,75	0,4352	180,00	54,0	0
7,357	16,75	0,4392	181,99	53,6	0
7,489	16,75	0,4472	184,00	53,2	0
7,547	16,75	0,4506	186,00	52,8	0
7,614	16,75	0,4546	188,00	52,3	0
7,734	16,75	0,4617	189,99	52,0	0

Peak hold step 3

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

7,817	16,75	0,4667	2,0000	51,5	0
7,839	16,75	0,4679	4,0040	51,1	0
7,977	16,75	0,4763	6,0080	50,7	0
8,055	16,75	0,4809	8,0120	50,3	0
8,100	16,75	0,4836	10,000	50,0	0
8,182	16,75	0,4884	12,004	49,7	0
8,255	16,75	0,4929	14,008	49,5	0
8,227	16,75	0,4911	16,012	49,3	0
8,284	16,75	0,4946	17,996	49,2	0
8,271	16,75	0,4938	20,004	49,2	0
8,319	16,75	0,4967	22,004	49,1	0
8,323	16,75	0,4969	24,008	49,1	0
8,338	16,75	0,4978	26,008	49,1	0
8,321	16,75	0,4968	28,012	49,1	0
8,329	16,75	0,4973	30,000	49,2	0
8,320	16,75	0,4967	31,996	49,2	0
8,341	16,75	0,4980	34,004	49,2	0
8,295	16,75	0,4951	36,004	49,3	0
8,316	16,75	0,4965	38,004	49,3	0
8,301	16,75	0,4956	40,004	49,3	0
8,281	16,75	0,4944	42,008	49,4	0
8,279	16,75	0,4943	44,004	49,4	0
8,307	16,75	0,4959	46,012	49,4	0
8,349	16,75	0,4985	48,008	49,4	0
8,273	16,75	0,4939	50,012	49,5	0
8,303	16,75	0,4957	51,996	49,5	0
8,277	16,75	0,4942	54,004	49,5	0
8,218	16,75	0,4906	56,008	49,5	0
8,249	16,75	0,4925	58,008	49,5	0
8,250	16,75	0,4925	60,008	49,6	0
8,137	16,75	0,4858	62,008	49,6	0
8,236	16,75	0,4917	63,996	49,6	0
8,250	16,75	0,4926	65,996	49,6	0
8,175	16,75	0,4880	67,996	49,7	0
8,139	16,75	0,4859	70,000	49,7	0
8,166	16,75	0,4874	72,000	49,7	0
8,121	16,75	0,4848	74,000	49,7	0
8,141	16,75	0,4860	76,004	49,7	0
8,186	16,75	0,4887	78,004	49,8	0
8,148	16,75	0,4865	80,004	49,8	0
8,129	16,75	0,4853	82,012	49,8	0
8,092	16,75	0,4831	84,008	49,8	0
8,101	16,75	0,4837	86,012	49,8	0
8,140	16,75	0,4860	88,012	49,8	0
8,070	16,75	0,4818	90,000	49,9	0
8,007	16,75	0,4780	92,000	49,9	0
8,056	16,75	0,4810	94,016	49,9	0
8,079	16,75	0,4823	96,016	49,9	0
8,041	16,75	0,4800	98,004	49,9	0
8,043	16,75	0,4802	100,00	49,9	0
8,079	16,75	0,4823	102,01	49,9	0
8,046	16,75	0,4803	104,02	49,9	0
8,027	16,75	0,4792	106,02	49,9	0
8,010	16,75	0,4782	108,00	49,9	0
8,007	16,75	0,4781	110,01	49,9	0
7,999	16,75	0,4776	112,00	50,0	0
8,046	16,75	0,4804	114,02	50,0	0
7,940	16,75	0,4739	116,02	50,0	0
7,957	16,75	0,4750	118,03	50,0	0
7,957	16,75	0,4751	120,02	50,0	0

Continuous ramp step

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

1,737	0,6647	2,614	4,9161	49,8	0
5,098	0,02753	185,2	15,008	47,4	0
8,437	0,03620	233,0	25,035	42,9	0
11,75	0,7846	14,98	34,996	38,6	0
15,07	33,64	0,4480	44,958	35,3	0
18,41	44,48	0,4139	54,985	33,7	0
21,75	58,39	0,3725	65,012	31,8	0
25,07	76,84	0,3262	74,973	29,6	0
28,41	87,55	0,3245	85,000	28,9	0
31,74	99,16	0,3201	95,027	29,4	0
35,06	129,3	0,2712	104,99	29,8	0
38,40	152,0	0,2526	115,02	29,9	0
41,74	181,9	0,2295	125,04	29,9	0
45,06	205,6	0,2192	135,00	29,9	0
48,37	231,1	0,2093	144,97	30,0	0
51,71	254,7	0,2030	154,99	30,0	0
55,05	266,0	0,2070	165,02	30,0	0
58,37	278,1	0,2099	174,98	30,0	0
61,71	296,3	0,2082	185,01	30,0	0
65,05	285,6	0,2277	195,04	30,0	0
68,36	299,2	0,2285	205,00	30,0	0

